A perdeuterated cryoprotectant for neutron studies and a demonstration of its use for neutron powder diffraction on L-(--)-ephedrine hemihydrate

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Standard

A perdeuterated cryoprotectant for neutron studies and a demonstration of its use for neutron powder diffraction on L-(--)-ephedrine hemihydrate. / Krebs, F. C.; Jørgensen, M.; Lebech, B.; Frydenvang, K.

I: Journal of Applied Crystallography, Bind 34, Nr. 2, 2001, s. 203-207.

Publikation: Bidrag til tidsskrift › Tidsskriftartikel › Forskning › fagfællebedømt

Harvard

Krebs, FC, Jørgensen, M, Lebech, B & Frydenvang, K 2001, 'A perdeuterated cryoprotectant for neutron studies and a demonstration of its use for neutron powder diffraction on L-(--)-ephedrine hemihydrate', Journal of Applied Crystallography, bind 34, nr. 2, s. 203-207. https://doi.org/10.1107/S0021889800018987

APA

Krebs, F. C., Jørgensen, M., Lebech, B., & Frydenvang, K. (2001). A perdeuterated cryoprotectant for neutron studies and a demonstration of its use for neutron powder diffraction on L-(--)-ephedrine hemihydrate. Journal of Applied Crystallography, 34(2), 203-207. https://doi.org/10.1107/S0021889800018987

Vancouver

Krebs FC, Jørgensen M, Lebech B, Frydenvang K. A perdeuterated cryoprotectant for neutron studies and a demonstration of its use for neutron powder diffraction on L-(--)-ephedrine hemihydrate. Journal of Applied Crystallography. 2001;34(2):203-207. https://doi.org/10.1107/S0021889800018987

Author

Krebs, F. C. ; Jørgensen, M. ; Lebech, B. ; Frydenvang, K. / A perdeuterated cryoprotectant for neutron studies and a demonstration of its use for neutron powder diffraction on L-(--)-ephedrine hemihydrate. I: Journal of Applied Crystallography. 2001 ; Bind 34, Nr. 2. s. 203-207.

Bibtex

@article{a241dd2d63174474be140197517a8b5f,
title = "A perdeuterated cryoprotectant for neutron studies and a demonstration of its use for neutron powder diffraction on L-(--)-ephedrine hemihydrate",
abstract = "The use of perdeuteropolyethylpropylene (d-PEP) as a cryoprotectant for neutron studies of molecular organic solids is demonstrated by the solution of the structure of L-(--)-ephedrine hemihydrate from neutron powder diffraction data on a sample containing 20 wt% d-PEP. It is demonstrated that no contribution from d-PEP to the scattering is observed. Neutron diffraction studies of solvent-containing molecular crystals that require a perdeuterated cryoprotectant oil are thus possible.",
author = "Krebs, {F. C.} and M. J{\o}rgensen and B. Lebech and K. Frydenvang",
year = "2001",
doi = "10.1107/S0021889800018987",
language = "English",
volume = "34",
pages = "203--207",
journal = "Journal of Applied Crystallography",
issn = "0021-8898",
publisher = "Wiley-Blackwell",
number = "2",

}

RIS

TY - JOUR

T1 - A perdeuterated cryoprotectant for neutron studies and a demonstration of its use for neutron powder diffraction on L-(--)-ephedrine hemihydrate

AU - Krebs, F. C.

AU - Jørgensen, M.

AU - Lebech, B.

AU - Frydenvang, K.

PY - 2001

Y1 - 2001

N2 - The use of perdeuteropolyethylpropylene (d-PEP) as a cryoprotectant for neutron studies of molecular organic solids is demonstrated by the solution of the structure of L-(--)-ephedrine hemihydrate from neutron powder diffraction data on a sample containing 20 wt% d-PEP. It is demonstrated that no contribution from d-PEP to the scattering is observed. Neutron diffraction studies of solvent-containing molecular crystals that require a perdeuterated cryoprotectant oil are thus possible.

AB - The use of perdeuteropolyethylpropylene (d-PEP) as a cryoprotectant for neutron studies of molecular organic solids is demonstrated by the solution of the structure of L-(--)-ephedrine hemihydrate from neutron powder diffraction data on a sample containing 20 wt% d-PEP. It is demonstrated that no contribution from d-PEP to the scattering is observed. Neutron diffraction studies of solvent-containing molecular crystals that require a perdeuterated cryoprotectant oil are thus possible.

UR - http://www.scopus.com/inward/record.url?scp=0035070855&partnerID=8YFLogxK

U2 - 10.1107/S0021889800018987

DO - 10.1107/S0021889800018987

M3 - Journal article

AN - SCOPUS:0035070855

VL - 34

SP - 203

EP - 207

JO - Journal of Applied Crystallography

JF - Journal of Applied Crystallography

SN - 0021-8898

IS - 2

ER -

ID: 382746969